Crystallography Open Database

Information card for entry 4073366

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Coordinates	4073366.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H69 Cl P2 Ru
Calculated formula	C36 H69 Cl P2 Ru
Title of publication	Activation of Chlorosilanes at Ruthenium: A Route to Silyl σ-Dihydrogen Complexes
Authors of publication	Lachaize, Sébastien; Caballero, Ana; Vendier, Laure; Sabo-Etienne, Sylviane
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	15
Pages of publication	3713
a	9.7161 ± 0.001 Å
b	10.1762 ± 0.0011 Å
c	10.6933 ± 0.001 Å
α	114.273 ± 0.011°
β	107.889 ± 0.011°
γ	90.735 ± 0.013°
Cell volume	905.3 ± 0.2 Å³
Cell temperature	160 K
Ambient diffraction temperature	180 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0531
Residual factor for significantly intense reflections	0.0367
Weighted residual factors for significantly intense reflections	0.0741
Weighted residual factors for all reflections included in the refinement	0.0785
Goodness-of-fit parameter for all reflections included in the refinement	0.953
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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