Information card for entry 4073395
| Formula |
C24 H33 F O5 Sn |
| Calculated formula |
C24 H33 F O5 Sn |
| Title of publication |
Ph(3-n)XnSnCH2-16-crown-5 (X = F, Cl, Br, I, SCN;n= 1, 2): Intramolecular O →Sn Coordination versus Ditopic Complexation of Sodium Thiocyanate† |
| Authors of publication |
Reeske, Gregor; Schürmann, Markus; Costisella, Burkhard; Jurkschat, Klaus |
| Journal of publication |
Organometallics |
| Year of publication |
2007 |
| Journal volume |
26 |
| Journal issue |
17 |
| Pages of publication |
4170 |
| a |
9.339 ± 0.001 Å |
| b |
10.7975 ± 0.0009 Å |
| c |
12.386 ± 0.002 Å |
| α |
97.413 ± 0.007° |
| β |
103.057 ± 0.005° |
| γ |
93.902 ± 0.006° |
| Cell volume |
1200.4 ± 0.3 Å3 |
| Cell temperature |
173 ± 1 K |
| Ambient diffraction temperature |
173 ± 1 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0363 |
| Residual factor for significantly intense reflections |
0.0282 |
| Weighted residual factors for significantly intense reflections |
0.0521 |
| Weighted residual factors for all reflections included in the refinement |
0.0531 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.956 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/4073395.html
