Crystallography Open Database

Information card for entry 4073418

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Coordinates	4073418.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C78 H0 N2 Tm2
Calculated formula	C78 H126 N2 Tm2
Title of publication	Synthesis and Reactivity of Organometallic Complexes of Divalent Thulium with Cyclopentadienyl and Phospholyl Ligands
Authors of publication	Jaroschik, Florian; Nief, François; Le Goff, Xavier-Frédéric; Ricard, Louis
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	14
Pages of publication	3552
a	10.447 ± 0.001 Å
b	10.865 ± 0.001 Å
c	18.222 ± 0.001 Å
α	106.818 ± 0.001°
β	91.546 ± 0.001°
γ	94.519 ± 0.001°
Cell volume	1971 ± 0.3 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0747
Residual factor for significantly intense reflections	0.0537
Weighted residual factors for significantly intense reflections	0.1411
Weighted residual factors for all reflections included in the refinement	0.1513
Goodness-of-fit parameter for all reflections included in the refinement	0.988
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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