Information card for entry 4073444

Structure parameters

• Formula: C35 H42 Cl2 F3 Fe2 N3 O7 S
• Calculated formula: C35 H42 Cl2 F3 Fe2 N3 O7 S
• Title of publication: Reactions of Diazo Compounds at μ-Vinyliminium Ligands: Synthesis of Novel Dinuclear Azine−Bis(alkylidene) Complexes
• Authors of publication: Busetto, Luigi; Marchetti, Fabio; Zacchini, Stefano; Zanotti, Valerio
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 14
• Pages of publication: 3577
• a: 11.814 ± 0.002 Å
• b: 12.577 ± 0.003 Å
• c: 15.404 ± 0.003 Å
• α: 107.03 ± 0.03°
• β: 98.26 ± 0.03°
• γ: 110.62 ± 0.03°
• Cell volume: 1968.8 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0828
• Residual factor for significantly intense reflections: 0.0607
• Weighted residual factors for significantly intense reflections: 0.1712
• Weighted residual factors for all reflections included in the refinement: 0.1901
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No