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Information card for entry 4073477
Preview
Coordinates | 4073477.cif |
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Original paper (by DOI) | HTML |
Formula | C27 H42 Cl O P2 Rh |
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Calculated formula | C27 H42 Cl1.46 P2 Rh |
Title of publication | Experimental and Computational Study of the Transformation of Terminal Alkynes to Vinylidene Ligands ontrans-(Chloro)bis(phosphine)Rh Fragments and Effects of Phosphine Substituents |
Authors of publication | Grotjahn, Douglas B.; Zeng, Xi; Cooksy, Andrew L.; Kassel, W. Scott; DiPasquale, Antonio G.; Zakharov, Lev. N.; Rheingold, Arnold L. |
Journal of publication | Organometallics |
Year of publication | 2007 |
Journal volume | 26 |
Journal issue | 14 |
Pages of publication | 3385 |
a | 10.232 ± 0.011 Å |
b | 15.409 ± 0.017 Å |
c | 9.569 ± 0.01 Å |
α | 90° |
β | 113.509 ± 0.015° |
γ | 90° |
Cell volume | 1383 ± 3 Å3 |
Cell temperature | 208 ± 2 K |
Ambient diffraction temperature | 208 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0498 |
Residual factor for significantly intense reflections | 0.0475 |
Weighted residual factors for significantly intense reflections | 0.1119 |
Weighted residual factors for all reflections included in the refinement | 0.1133 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.089 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4073477.html
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