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Information card for entry 4073531
Preview
Coordinates | 4073531.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C47 H47 B N4 O0.5 P2 Rh S3 |
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Calculated formula | C47 H47 B N4 O0.5 P2 Rh S3 |
Title of publication | Metallaboratranes: The M→B Dative Bond as a Ligand Activating Function in the Phosphaboration of Carbon Monosulfide† |
Authors of publication | Crossley, Ian R.; Hill, Anthony F.; Willis, Anthony C. |
Journal of publication | Organometallics |
Year of publication | 2007 |
Journal volume | 26 |
Journal issue | 16 |
Pages of publication | 3891 |
a | 12.8506 ± 0.0005 Å |
b | 13.0843 ± 0.0006 Å |
c | 13.9351 ± 0.0006 Å |
α | 85.869 ± 0.003° |
β | 83.163 ± 0.003° |
γ | 75.657 ± 0.002° |
Cell volume | 2251.68 ± 0.17 Å3 |
Cell temperature | 200 K |
Ambient diffraction temperature | 200 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0535 |
Residual factor for significantly intense reflections | 0.0336 |
Weighted residual factors for all reflections | 0.0416 |
Weighted residual factors for significantly intense reflections | 0.0344 |
Weighted residual factors for all reflections included in the refinement | 0.0344 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.1399 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4073531.html
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Users of the data should acknowledge the original authors of the
structural data.