Information card for entry 4073533

Structure parameters

• Formula: C48 H50 Cl4 O8 Sb6
• Calculated formula: C48 H50 Cl4 O8 Sb6
• Title of publication: The First Mixed-Valent Antimony(III/V) Oxo Clusters (2,6-Mes2C6H3Sb)2(ClSb)4O8and (2,6-Mes2C6H3Sb)4(ClSb)4(HOSb)2O14†
• Authors of publication: Beckmann, Jens; Heek, Timm; Takahashi, Masashi
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 15
• Pages of publication: 3633
• a: 8.791 ± 0.0007 Å
• b: 21.8251 ± 0.0012 Å
• c: 14.2469 ± 0.0011 Å
• α: 90°
• β: 100.473 ± 0.006°
• γ: 90°
• Cell volume: 2687.9 ± 0.3 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0532
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0798
• Weighted residual factors for all reflections included in the refinement: 0.0852
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No