Information card for entry 4073679

Structure parameters

• Formula: C47 H64.5 N2 O4.25 Si2 Zr
• Calculated formula: C47 H42 N2 O4.25 Si2 Zr
• Title of publication: A Discrete Ortho-Lithiated Acetophenone Imine Derivative: Isolation, Characterization, and Synthesis of Group IV Metal Complexes
• Authors of publication: Baiz, Tamam I.; Schmidt, Joseph A. R.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 17
• Pages of publication: 4094
• a: 11.4685 ± 0.0006 Å
• b: 12.6056 ± 0.0006 Å
• c: 18.3425 ± 0.0009 Å
• α: 81.983 ± 0.001°
• β: 77.081 ± 0.001°
• γ: 65.461 ± 0.001°
• Cell volume: 2347.9 ± 0.2 ų
• Cell temperature: 135 ± 2 K
• Ambient diffraction temperature: 135 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1291
• Residual factor for significantly intense reflections: 0.07
• Weighted residual factors for significantly intense reflections: 0.182
• Weighted residual factors for all reflections included in the refinement: 0.2098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No