Crystallography Open Database

Information card for entry 4073761

Preview

Coordinates	4073761.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H46 Os Ru
Calculated formula	C35 H46 Os Ru
Title of publication	Reaction of a Heterobimetallic Polyhydrido Cluster, [CpRu(μ-H)4OsCp] (Cp* = η5-C5Me5), with Diphenylacetylene. Regioselective C−H Bond Activation at the Osmium Center
Authors of publication	Shima, Takanori; Ichikawa, Toshiaki; Suzuki, Hiroharu
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	25
Pages of publication	6329
a	9.0941 ± 0.0012 Å
b	17.826 ± 0.002 Å
c	19.7889 ± 0.0019 Å
α	90°
β	94.333 ± 0.004°
γ	90°
Cell volume	3198.8 ± 0.6 Å³
Cell temperature	233 ± 2 K
Ambient diffraction temperature	233 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0994
Residual factor for significantly intense reflections	0.0789
Weighted residual factors for significantly intense reflections	0.1876
Weighted residual factors for all reflections included in the refinement	0.1953
Goodness-of-fit parameter for all reflections included in the refinement	1.142
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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