Crystallography Open Database

Information card for entry 4073763

Preview

Coordinates	4073763.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H42 Os Ru
Calculated formula	C34 H42 Os Ru
Title of publication	Reaction of a Heterobimetallic Polyhydrido Cluster, [CpRu(μ-H)4OsCp] (Cp* = η5-C5Me5), with Diphenylacetylene. Regioselective C−H Bond Activation at the Osmium Center
Authors of publication	Shima, Takanori; Ichikawa, Toshiaki; Suzuki, Hiroharu
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	25
Pages of publication	6329
a	11.604 ± 0.002 Å
b	16.869 ± 0.003 Å
c	15.809 ± 0.003 Å
α	90°
β	104.89 ± 0.03°
γ	90°
Cell volume	2990.7 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0367
Residual factor for significantly intense reflections	0.0324
Weighted residual factors for significantly intense reflections	0.0757
Weighted residual factors for all reflections included in the refinement	0.0772
Goodness-of-fit parameter for all reflections included in the refinement	1.133
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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