Crystallography Open Database

Information card for entry 4073821

Preview

Coordinates	4073821.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H44 Cl8 N2 P2 Ru
Calculated formula	C45.589 H43.178 Cl7.178 N2 P2 Ru
Title of publication	[RuCl2(PPh3)(PNN‘)] Complexes as Efficient Catalysts in Transfer Hydrogenation of Ketones
Authors of publication	Del Zotto, Alessandro; Baratta, Walter; Ballico, Maurizio; Herdtweck, Eberhardt; Rigo, Pierluigi
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	23
Pages of publication	5636
a	37.2956 ± 0.001 Å
b	9.9079 ± 0.0003 Å
c	24.8352 ± 0.0005 Å
α	90°
β	90.938 ± 0.002°
γ	90°
Cell volume	9175.9 ± 0.4 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.081
Residual factor for significantly intense reflections	0.0686
Weighted residual factors for significantly intense reflections	0.1654
Weighted residual factors for all reflections included in the refinement	0.1693
Goodness-of-fit parameter for all reflections included in the refinement	1.192
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4073821.html