Information card for entry 4073849

Structure parameters

• Formula: C32 H58 Li O2 Si4 Tb
• Calculated formula: C32 H58 Li O2 Si4 Tb
• Title of publication: A Surprising Solvent Effect on the Crystal Structure of an Anionic Lanthanide Sandwich Complex†
• Authors of publication: Lorenz, Volker; Edelmann, Anja; Blaurock, Steffen; Freise, Fritjof; Edelmann, Frank T.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 26
• Pages of publication: 6681
• a: 11.851 ± 0.002 Å
• b: 16.094 ± 0.003 Å
• c: 20.411 ± 0.004 Å
• α: 90°
• β: 97.04 ± 0.03°
• γ: 90°
• Cell volume: 3863.6 ± 1.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0798
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.0903
• Weighted residual factors for all reflections included in the refinement: 0.0977
• Goodness-of-fit parameter for all reflections included in the refinement: 0.844
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No