Information card for entry 4073852

Structure parameters

• Formula: C67 H60 D9 Sb2 Ti
• Calculated formula: C67 H60 D9 Sb2 Ti
• Title of publication: Syntheses and Structures of Distibene Complexes of Tungsten and Titanium: [W(CO)5{(2,6-Mes2C6H3)2Sb2}] (Mes = 2,4,6-Me3C6H2) and [Cp2Ti{(2,6-Mes2C6H3)2Sb2)}]
• Authors of publication: Breunig, Hans J.; Borrmann, Tobias; Lork, Enno; Raţ, Ciprian I.; Rosenthal, Uwe
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 22
• Pages of publication: 5364
• a: 11.272 ± 0.001 Å
• b: 12.836 ± 0.002 Å
• c: 20.263 ± 0.002 Å
• α: 97.06 ± 0.01°
• β: 93.69 ± 0.01°
• γ: 109.12 ± 0.01°
• Cell volume: 2731.9 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0735
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.088
• Weighted residual factors for all reflections included in the refinement: 0.0983
• Goodness-of-fit parameter for all reflections included in the refinement: 0.976
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No