Information card for entry 4073863

Structure parameters

• Formula: C22 H30 Cl2 O4 Rh2
• Calculated formula: C22 H30 Cl2 O4 Rh2
• SMILES: C12=[O][Rh]3456([c]7([c]3([c]4([c]5([c]67C)C)C)C)C)(OC2=[O][Rh]2345([c]6([c]2([c]3([c]4([c]56C)C)C)C)C)(O1)Cl)Cl
• Title of publication: Stepwise Formation of Tetra- and Hexanuclear Iridium and Rhodium Complexes Containing Oxalato Ligands
• Authors of publication: Han, Ying-Feng; Lin, Yue-Jian; Jia, Wei-Guo; Weng, Lin-Hong; Jin, Guo-Xin
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 24
• Pages of publication: 5848
• a: 8.387 ± 0.003 Å
• b: 8.827 ± 0.003 Å
• c: 16.629 ± 0.006 Å
• α: 90°
• β: 93.999 ± 0.005°
• γ: 90°
• Cell volume: 1228.1 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0558
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.0963
• Weighted residual factors for all reflections included in the refinement: 0.1016
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No