Information card for entry 4073928

Structure parameters

• Formula: C40 H33 N2 O10 Os4
• Calculated formula: C40 H33 N2 O10 Os4
• Title of publication: Normal and Abnormal NHC Coordination in [Os4(μ-H)4(CO)11(IMes)] and Exhaustive Dehydrogenation of an IMes Methyl Group
• Authors of publication: Cooke, Craig E.; Jennings, Michael C.; Pomeroy, Roland K.; Clyburne, Jason A. C.
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 25
• Pages of publication: 6059
• a: 12.3074 ± 0.0004 Å
• b: 12.6819 ± 0.0004 Å
• c: 14.7598 ± 0.0005 Å
• α: 74.792 ± 0.002°
• β: 87.235 ± 0.002°
• γ: 62.317 ± 0.002°
• Cell volume: 1961.26 ± 0.12 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0552
• Residual factor for significantly intense reflections: 0.0513
• Weighted residual factors for significantly intense reflections: 0.1408
• Weighted residual factors for all reflections included in the refinement: 0.1448
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No