Information card for entry 4074177

Structure parameters

• Formula: C84 H66 B F24 Ge P Ru S2
• Calculated formula: C84 H66 B F24 Ge P Ru S2
• Title of publication: Synthesis of Oxo- and Sulfido-Bridged Germanium−Ruthenium Complexes and Reactions on the Chalcogenido Bridges
• Authors of publication: Matsumoto, Tsuyoshi; Nakaya, Yukiko; Tatsumi, Kazuyuki
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 20
• Pages of publication: 4835
• a: 20.77 ± 0.004 Å
• b: 12.102 ± 0.002 Å
• c: 31.916 ± 0.006 Å
• α: 90°
• β: 95.255 ± 0.003°
• γ: 90°
• Cell volume: 7989 ± 3 ų
• Cell temperature: 173.1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for all reflections included in the refinement: 0.1133
• Goodness-of-fit parameter for all reflections included in the refinement: 0.922
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No