Crystallography Open Database

Information card for entry 4074179

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Coordinates	4074179.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C87.5 H70 B F24 Ge O P Ru S
Calculated formula	C87.5 H66 B F24 Ge O P Ru S
Title of publication	Synthesis of Oxo- and Sulfido-Bridged Germanium−Ruthenium Complexes and Reactions on the Chalcogenido Bridges
Authors of publication	Matsumoto, Tsuyoshi; Nakaya, Yukiko; Tatsumi, Kazuyuki
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	20
Pages of publication	4835
a	12.5318 ± 0.0015 Å
b	17.246 ± 0.002 Å
c	19.56 ± 0.003 Å
α	84.988 ± 0.004°
β	84.367 ± 0.004°
γ	75.79 ± 0.003°
Cell volume	4069.5 ± 0.9 Å³
Cell temperature	123.1 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0413
Weighted residual factors for all reflections included in the refinement	0.054
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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