Crystallography Open Database

Information card for entry 4074184

Preview

Coordinates	4074184.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C82 H70 Li4 N6 P4 S8
Calculated formula	C82 H70 Li4 N6 P4 S8
Title of publication	Phosphorus-Stabilized Geminal Dianions
Authors of publication	Cantat, Thibault; Ricard, Louis; Le Floch, Pascal; Mézailles, Nicolas
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	21
Pages of publication	4965
a	18.156 ± 0.001 Å
b	19.21 ± 0.001 Å
c	24.037 ± 0.001 Å
α	90°
β	108.434 ± 0.001°
γ	90°
Cell volume	7953.4 ± 0.7 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0667
Residual factor for significantly intense reflections	0.051
Weighted residual factors for significantly intense reflections	0.1362
Weighted residual factors for all reflections included in the refinement	0.1464
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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