Information card for entry 4074201

Structure parameters

• Chemical name: Tetrakis-(3,4-dichloro-phenyl)stannane
• Formula: C24 H12 Cl8 Sn
• Calculated formula: C24 H12 Cl8 Sn
• SMILES: [Sn](c1cc(Cl)c(Cl)cc1)(c1cc(Cl)c(Cl)cc1)(c1cc(Cl)c(Cl)cc1)c1cc(Cl)c(Cl)cc1
• Title of publication: The Ullmann Coupling Reaction: A New Approach to Tetraarylstannanes
• Authors of publication: Shaikh, Nadim S.; Parkin, Sean; Lehmler, Hans-Joachim
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 17
• Pages of publication: 4207
• a: 9.8948 ± 0.0001 Å
• b: 11.2574 ± 0.0002 Å
• c: 11.7771 ± 0.0002 Å
• α: 97.9527 ± 0.0006°
• β: 98.0515 ± 0.0006°
• γ: 94.0355 ± 0.0007°
• Cell volume: 1281.02 ± 0.03 ų
• Cell temperature: 90 ± 0.2 K
• Ambient diffraction temperature: 90 ± 0.2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0339
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0537
• Weighted residual factors for all reflections included in the refinement: 0.0573
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No