Information card for entry 4074210

Structure parameters

• Formula: C28 H33 Os P
• Calculated formula: C28 H33 Os P
• SMILES: [OsH3]1234([P](c5ccccc5)(c5ccccc5)c5ccccc5)[c]5([c]4([c]3([c]2([c]15C)C)C)C)C
• Title of publication: Synthesis and Characterization of Osmium(IV) Polyhydride Complexes of Stoichiometry (C5Me5)OsH3(L). Crystal Structures of (C5Me5)OsH3(AsPh3) and (C5Me5)OsH3(PPh3)
• Authors of publication: Gross, Christopher L.; Girolami, Gregory S.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 20
• Pages of publication: 4792
• a: 9.0638 ± 0.0001 Å
• b: 9.1459 ± 0.0002 Å
• c: 16.6003 ± 0.0001 Å
• α: 94.827 ± 0.001°
• β: 101.359 ± 0.001°
• γ: 115.217 ± 0.001°
• Cell volume: 1198.47 ± 0.03 ų
• Cell temperature: 198 ± 2 K
• Ambient diffraction temperature: 198 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0244
• Residual factor for significantly intense reflections: 0.0221
• Weighted residual factors for significantly intense reflections: 0.0524
• Weighted residual factors for all reflections included in the refinement: 0.0542
• Goodness-of-fit parameter for all reflections included in the refinement: 1.102
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No