Information card for entry 4074229

Structure parameters

• Chemical name: (K-crypt)6[Pb9Zn(C6H5)]2*2en*tol
• Formula: C131 H250 K6 N16 O36 Pb18 Zn2
• Calculated formula: C131 H250.04 K6 N16 O36 Pb18 Zn2
• Title of publication: Organozinc Derivatives of Deltahedral Zintl Ions: Synthesis and Characterization ofcloso-[E9Zn(C6H5)]3-(E = Si, Ge, Sn, Pb)
• Authors of publication: Goicoechea, Jose M.; Sevov, Slavi C.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 19
• Pages of publication: 4530
• a: 15.8267 ± 0.0004 Å
• b: 22.446 ± 0.0007 Å
• c: 27.5057 ± 0.0008 Å
• α: 87.793 ± 0.002°
• β: 74.942 ± 0.002°
• γ: 89.428 ± 0.002°
• Cell volume: 9428.8 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0657
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.1011
• Weighted residual factors for all reflections included in the refinement: 0.109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No