Information card for entry 4074359

Structure parameters

• Formula: C53 H70 Cl N3 O2 P Rh
• Calculated formula: C53 H70 Cl N3 O2 P Rh
• Title of publication: Rhodium(III) Peroxo Complexes Containing Carbene and Phosphine Ligands
• Authors of publication: Yu, Xiao-Yan; Patrick, Brian O.; James, Brian R.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 20
• Pages of publication: 4870
• a: 14.684 ± 0.002 Å
• b: 16.898 ± 0.002 Å
• c: 19.798 ± 0.002 Å
• α: 90°
• β: 90.927 ± 0.008°
• γ: 90°
• Cell volume: 4911.8 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0907
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.0549
• Weighted residual factors for all reflections included in the refinement: 0.0613
• Goodness-of-fit parameter for all reflections included in the refinement: 0.822
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No