Information card for entry 4074387

Structure parameters

• Formula: C9 H27 B P Rb Si2
• Calculated formula: C9 H27 B P Rb Si2
• Title of publication: Heavier Alkali Metal Complexes of a Silicon- and Phosphine-Borane-Stabilized Carbanion
• Authors of publication: Izod, Keith; Wills, Corinne; Clegg, William; Harrington, Ross W.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 22
• Pages of publication: 5326
• a: 16.216 ± 0.002 Å
• b: 13.691 ± 0.003 Å
• c: 16.924 ± 0.003 Å
• α: 90°
• β: 113.387 ± 0.012°
• γ: 90°
• Cell volume: 3448.7 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0949
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.0642
• Weighted residual factors for all reflections included in the refinement: 0.0771
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No