Information card for entry 4074397

Structure parameters

• Chemical name: Ti(NiPr)(Me3[9]aneN3)Me2 . 0.5 C6H6
• Formula: C17 H37 N4 Ti
• Calculated formula: C17 H37 N4 Ti
• Title of publication: Synthesis and Ethylene Polymerization Capability of Metallocene-like Imido Titanium Dialkyl Compounds and Their Reactions with AliBu3
• Authors of publication: Bolton, Paul D.; Adams, Nico; Clot, Eric; Cowley, Andrew R.; Wilson, Paul J.; Schröder, Martin; Mountford, Philip
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 23
• Pages of publication: 5549
• a: 35.1006 ± 0.0008 Å
• b: 8.354 ± 0.0002 Å
• c: 13.6754 ± 0.0004 Å
• α: 90°
• β: 95.7541 ± 0.0008°
• γ: 90°
• Cell volume: 3989.84 ± 0.18 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0417
• Weighted residual factors for all reflections included in the refinement: 0.0238
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0661
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No