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Information card for entry 4074427
Preview
Coordinates | 4074427.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C83.5 H85 O P5 Pt2 |
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Calculated formula | C73 H72 O P5 Pt2 |
SMILES | [Pt]1([P](CC[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)([P]([Pt]1([P](CC[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)C)(c1ccccc1)c1ccccc1)C.O.Cc1ccccc1 |
Title of publication | P−C and C−C Bond Formation by Michael Addition in Platinum-Catalyzed Hydrophosphination and in the Stoichiometric Reactions of Platinum Phosphido Complexes with Activated Alkenes |
Authors of publication | Scriban, Corina; Glueck, David S.; Zakharov, Lev N.; Kassel, W. Scott; DiPasquale, Antonio G.; Golen, James A.; Rheingold, Arnold L. |
Journal of publication | Organometallics |
Year of publication | 2006 |
Journal volume | 25 |
Journal issue | 24 |
Pages of publication | 5757 |
a | 13.0614 ± 0.0012 Å |
b | 16.8404 ± 0.0015 Å |
c | 17.8216 ± 0.0016 Å |
α | 105.327 ± 0.001° |
β | 110.081 ± 0.001° |
γ | 91.999 ± 0.001° |
Cell volume | 3516.4 ± 0.6 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0474 |
Residual factor for significantly intense reflections | 0.0387 |
Weighted residual factors for significantly intense reflections | 0.1057 |
Weighted residual factors for all reflections included in the refinement | 0.1104 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.045 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4074427.html
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Users of the data should acknowledge the original authors of the
structural data.