Information card for entry 4074534

Structure parameters

• Formula: C72 H64.5 Ag4 Au3 Cl0.5 Fe6 O5.5
• Calculated formula: C72 H54 Ag4 Au3 Cl0.5 Fe6 O5.5
• Title of publication: Rhombic Dodecahedral Ag8M6(M = Cu, Ag, Au) Cluster Complexes of Ferrocenylethynyl Prepared by Reaction of (AgC⋮CFc)nwith [M2(Ph2PNHPh2)2(MeCN)2]2+(M = Cu, Ag, Au)
• Authors of publication: Wei, Qiao-Hua; Yin, Gang-Qiang; Zhang, Li-Yi; Chen, Zhong-Ning
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 21
• Pages of publication: 4941
• a: 15.6892 ± 0.0001 Å
• b: 16.7712 ± 0.0003 Å
• c: 17.7327 ± 0.0003 Å
• α: 81.126 ± 0.001°
• β: 68.883 ± 0.001°
• γ: 62.678 ± 0.001°
• Cell volume: 3866.69 ± 0.11 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1473
• Residual factor for significantly intense reflections: 0.0986
• Weighted residual factors for significantly intense reflections: 0.253
• Weighted residual factors for all reflections included in the refinement: 0.3117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.228
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No