Information card for entry 4074552

Structure parameters

• Formula: C33 H27 Al2 F18 N3 P
• Calculated formula: C33 H27 Al2 F18 N3 P
• Title of publication: Ligand Design for the Assembly of Polynuclear Complexes: Syntheses and Structures of Trinuclear and Tetranuclear Aluminum Alkyl Complexes Bearing Tripodal Diamidoselenophosphinito Ligands and a Comparison to Related Tripodal Triamidophosphine Complexes
• Authors of publication: Han, Hua; Johnson, Samuel A.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 23
• Pages of publication: 5594
• a: 11.2709 ± 0.0015 Å
• b: 11.6947 ± 0.0015 Å
• c: 15.652 ± 0.002 Å
• α: 68.451 ± 0.001°
• β: 86.064 ± 0.001°
• γ: 78.921 ± 0.001°
• Cell volume: 1883.1 ± 0.4 ų
• Cell temperature: 446 ± 2 K
• Ambient diffraction temperature: 446 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0685
• Residual factor for significantly intense reflections: 0.0601
• Weighted residual factors for significantly intense reflections: 0.165
• Weighted residual factors for all reflections included in the refinement: 0.1747
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No