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Information card for entry 4074581
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Coordinates | 4074581.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | complex 2a |
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Chemical name | complex 2a |
Formula | C30 H36 Fe N2 O Si |
Calculated formula | C30 H36 Fe N2 O Si |
SMILES | [Fe]1234([Si](N(c5ccccc5)c5ccccc5)(C)C)([n]5ccccc5)(C#[O])[c]5([c]1([c]2([c]3([c]45C)C)C)C)C |
Title of publication | Insertion of Pyridine into an Iron−Silicon Bond and Photochemical Conversion of the Insertion Product Cp*(OC)Fe{η3(C,C,C)-C5H5NSiMe2NPh2} to a Sandwich Compound |
Authors of publication | Iwata, Masatoshi; Okazaki, Masaaki; Tobita, Hiromi |
Journal of publication | Organometallics |
Year of publication | 2006 |
Journal volume | 25 |
Journal issue | 26 |
Pages of publication | 6115 |
a | 11.4245 ± 0.0004 Å |
b | 16.9079 ± 0.0005 Å |
c | 13.866 ± 0.0003 Å |
α | 90° |
β | 92.431 ± 0.002° |
γ | 90° |
Cell volume | 2676.01 ± 0.14 Å3 |
Cell temperature | 150.2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for significantly intense reflections | 0.033 |
Weighted residual factors for all reflections included in the refinement | 0.1193 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.988 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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