Crystallography Open Database

Information card for entry 4074699

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Coordinates	4074699.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H54 Cl5 Fe4 Ni2 P4
Calculated formula	C65 H54 Cl5 Fe4 Ni2 P4
Title of publication	Stereoselective Synthesis and Coordination Behavior of Phosphorus-Bridged [1.1]Ferrocenophanes
Authors of publication	Imamura, Yuki; Mizuta, Tsutomu; Miyoshi, Katsuhiko
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	4
Pages of publication	882
a	10.076 ± 0.0001 Å
b	16.395 ± 0.0002 Å
c	18.024 ± 0.0003 Å
α	95.883 ± 0.001°
β	100.267 ± 0.001°
γ	92.234 ± 0.001°
Cell volume	2909.4 ± 0.07 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0773
Residual factor for significantly intense reflections	0.054
Weighted residual factors for significantly intense reflections	0.1128
Weighted residual factors for all reflections included in the refinement	0.1223
Goodness-of-fit parameter for all reflections included in the refinement	1.174
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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