Information card for entry 4074701

Structure parameters

• Chemical name: 1,1,1,1-[ethylene-N,N'-bis(2-oxy-4-methoxybenzophenone)iminato]- 2,5-diphenyl-2,5-diazasilolidine dioxane solvate
• Formula: C52 H56 N4 O8 Si
• Calculated formula: C52 H56 N4 O8 Si
• Title of publication: Intramolecular Interligand Charge Transfer in Hexacoordinate Silicon Complexes
• Authors of publication: Wagler, Jörg; Gerlach, Daniela; Böhme, Uwe; Roewer, Gerhard
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 12
• Pages of publication: 2929
• a: 12.618 ± 0.001 Å
• b: 13.826 ± 0.001 Å
• c: 14.102 ± 0.001 Å
• α: 96.355 ± 0.01°
• β: 109.511 ± 0.01°
• γ: 97.251 ± 0.01°
• Cell volume: 2269.4 ± 0.3 ų
• Cell temperature: 198 ± 2 K
• Ambient diffraction temperature: 198 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.088
• Weighted residual factors for all reflections included in the refinement: 0.0999
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No