Crystallography Open Database

Information card for entry 4074831

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Coordinates	4074831.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H28 Cl N2 O4 P Pd
Calculated formula	C27 H28 Cl N2 O4 P Pd
Title of publication	Synthesis, Characterization, and Transition-Metal Complexes of 3,4-Diazaphospholanes
Authors of publication	Landis, Clark R.; Nelson, Ryan C.; Jin, Wiechang; Bowman, Amanda C.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	6
Pages of publication	1377 - 1391
a	9.5131 ± 0.0003 Å
b	10.7018 ± 0.0004 Å
c	13.63 ± 0.0005 Å
α	86.154 ± 0.001°
β	83.448 ± 0.001°
γ	81.095 ± 0.001°
Cell volume	1360.23 ± 0.08 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0356
Residual factor for significantly intense reflections	0.034
Weighted residual factors for significantly intense reflections	0.091
Weighted residual factors for all reflections included in the refinement	0.0924
Goodness-of-fit parameter for all reflections included in the refinement	1.009
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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