Information card for entry 4074838

Structure parameters

• Formula: C46.5 H64 Al N3
• Calculated formula: C46.5 H60 Al N3
• Title of publication: Reaction of the Diimine Pyridine Ligand with Aluminum Alkyls: An Unexpectedly Complex Reaction
• Authors of publication: Knijnenburg, Quinten; Smits, Jan M. M.; Budzelaar, Peter H. M.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 4
• Pages of publication: 1036
• a: 9.6818 ± 0.0006 Å
• b: 10.8761 ± 0.0007 Å
• c: 21.6405 ± 0.0017 Å
• α: 100.973 ± 0.006°
• β: 99.38 ± 0.005°
• γ: 104.004 ± 0.005°
• Cell volume: 2117.7 ± 0.3 ų
• Cell temperature: 208 ± 2 K
• Ambient diffraction temperature: 208 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.122
• Residual factor for significantly intense reflections: 0.0701
• Weighted residual factors for all reflections: 0.1802
• Weighted residual factors for significantly intense reflections: 0.1544
• Weighted residual factors for all reflections included in the refinement: 0.1802
• Goodness-of-fit parameter for all reflections: 1.032
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No