Information card for entry 4074842

Structure parameters

• Formula: C44 H69 Al N3
• Calculated formula: C44 H69 Al N3
• Title of publication: Reaction of the Diimine Pyridine Ligand with Aluminum Alkyls: An Unexpectedly Complex Reaction
• Authors of publication: Knijnenburg, Quinten; Smits, Jan M. M.; Budzelaar, Peter H. M.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 4
• Pages of publication: 1036
• a: 13.1131 ± 0.0015 Å
• b: 14.23 ± 0.002 Å
• c: 22.256 ± 0.003 Å
• α: 90°
• β: 94.088 ± 0.01°
• γ: 90°
• Cell volume: 4142.4 ± 0.9 ų
• Cell temperature: 208 ± 2 K
• Ambient diffraction temperature: 208 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2387
• Residual factor for significantly intense reflections: 0.1456
• Weighted residual factors for all reflections: 0.2946
• Weighted residual factors for significantly intense reflections: 0.2523
• Weighted residual factors for all reflections included in the refinement: 0.2946
• Goodness-of-fit parameter for all reflections: 1.131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No