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Information card for entry 4074910
Preview
Coordinates | 4074910.cif |
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Original paper (by DOI) | HTML |
Formula | C53 H107 Cl2 Hf Li N4 Si6 |
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Calculated formula | C53 H107 Cl2 Hf Li N4 Si6 |
Title of publication | Reduction of Tetravalent Group 4 Metal Complexes Supported by an Extremely Bulky, Unsymmetrically Substituted β-Diketiminato Ligand Leading to the Regioselective CN Bond Cleavage Giving Ring-Contracted Metal-Imido Complexes |
Authors of publication | Hamaki, Hirofumi; Takeda, Nobuhiro; Tokitoh, Norihiro |
Journal of publication | Organometallics |
Year of publication | 2006 |
Journal volume | 25 |
Journal issue | 10 |
Pages of publication | 2457 |
a | 12.6966 ± 0.0017 Å |
b | 15.754 ± 0.002 Å |
c | 19.249 ± 0.003 Å |
α | 72.09 ± 0.005° |
β | 69.348 ± 0.004° |
γ | 77.721 ± 0.006° |
Cell volume | 3404.7 ± 0.8 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0249 |
Residual factor for significantly intense reflections | 0.0225 |
Weighted residual factors for significantly intense reflections | 0.0487 |
Weighted residual factors for all reflections included in the refinement | 0.0498 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4074910.html
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