Crystallography Open Database

Information card for entry 4075036

Preview

Coordinates	4075036.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H16 O11 Os3 Sn
Calculated formula	C29 H16 O11 Os3 Sn
Title of publication	A New Tris(diphenylstannylene)triosmium Carbonyl Cluster Complex and Its Reactions with Pt(PBut3)2and Pt(PPh3)4
Authors of publication	Adams, Richard D.; Captain, Burjor; Zhu, Lei
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	8
Pages of publication	2049
a	9.0694 ± 0.0002 Å
b	16.4421 ± 0.0004 Å
c	23.2581 ± 0.0006 Å
α	71.65°
β	81.103 ± 0.001°
γ	85.317 ± 0.001°
Cell volume	3250.27 ± 0.14 Å³
Cell temperature	294 ± 2 K
Ambient diffraction temperature	294 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0489
Residual factor for significantly intense reflections	0.0322
Weighted residual factors for significantly intense reflections	0.0769
Weighted residual factors for all reflections included in the refinement	0.0856
Goodness-of-fit parameter for all reflections included in the refinement	1.007
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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