Information card for entry 4075044

Structure parameters

• Formula: C72 H124 N4 O8 P8 Rh4
• Calculated formula: C72 H124 N4 O8 P8 Rh4
• Title of publication: Exclusive C−C Activation and an Apparent α-H Elimination with a Rhodium Phosphinite Pincer Complex
• Authors of publication: Salem, Hiyam; Ben-David, Yehoshoa; Shimon, Linda J. W.; Milstein, David
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 9
• Pages of publication: 2292
• a: 13.925 ± 0.003 Å
• b: 17.773 ± 0.004 Å
• c: 36.02 ± 0.007 Å
• α: 90°
• β: 94.03 ± 0.03°
• γ: 90°
• Cell volume: 8893 ± 3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0969
• Residual factor for significantly intense reflections: 0.0792
• Weighted residual factors for significantly intense reflections: 0.1959
• Weighted residual factors for all reflections included in the refinement: 0.205
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No