Information card for entry 4075055

Structure parameters

• Common name: [{-CH2PPhC(NiPr)(NHiPr)}2]
• Formula: C28 H44 N4 P2
• Calculated formula: C28 H44 N4 P2
• Title of publication: Coordination Chemistry of Isomeric Mixtures of Linked Di(phosphaguanidine) Compounds: A Spectroscopic and Crystallographic Study
• Authors of publication: Mansfield, Natalie E.; Coles, Martyn P.; Avent, Anthony G.; Hitchcock, Peter B.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 10
• Pages of publication: 2470
• a: 11.52 ± 0.0007 Å
• b: 11.938 ± 0.0007 Å
• c: 12.5195 ± 0.001 Å
• α: 83.491 ± 0.003°
• β: 90.327 ± 0.003°
• γ: 63.088 ± 0.003°
• Cell volume: 1522.23 ± 0.18 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0803
• Residual factor for significantly intense reflections: 0.0543
• Weighted residual factors for significantly intense reflections: 0.1149
• Weighted residual factors for all reflections included in the refinement: 0.1259
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No