Oxidation of the Bis-molybdenum(0) Trianion [1,3,6-{Mo(CO)3}-3,6-(μ-H)2-1,1,1-(CO)3-2-Ph-closo-1,2-MoCB9H7]3-: Metal and Boron Vertex Substitution and Cluster Expansion§
Authors of publication
Lei, Peng; McGrath, Thomas D.; Stone, F. Gordon A.
Journal of publication
Organometallics
Year of publication
2006
Journal volume
25
Journal issue
8
Pages of publication
2011
a
14.867 ± 0.003 Å
b
17.634 ± 0.003 Å
c
17.202 ± 0.003 Å
α
90°
β
90°
γ
90°
Cell volume
4509.8 ± 1.4 Å3
Cell temperature
110 ± 2 K
Ambient diffraction temperature
110 ± 2 K
Number of distinct elements
5
Space group number
36
Hermann-Mauguin space group symbol
C m c 21
Hall space group symbol
C 2c -2
Residual factor for all reflections
0.0472
Residual factor for significantly intense reflections
0.0373
Weighted residual factors for significantly intense reflections
0.0907
Weighted residual factors for all reflections included in the refinement
0.0946
Goodness-of-fit parameter for all reflections included in the refinement
