Information card for entry 4075118

Structure parameters

• Formula: C46.6 H51.2 Cl1.2 O3 P2 S Sn
• Calculated formula: C46.6 H50 Cl1.2 O3 P2 S Sn
• Title of publication: The First O,C,S-Coordinating Pincer-Type Ligand and Its Application to the Synthesis of a Triorganotin Cation Stabilized by Two Different Donor Atoms†
• Authors of publication: Fischer, Jan; Schürmann, Markus; Mehring, Michael; Zachwieja, Uwe; Jurkschat, Klaus
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 11
• Pages of publication: 2886
• a: 12.3286 ± 0.0009 Å
• b: 13.3439 ± 0.0008 Å
• c: 15.2367 ± 0.0008 Å
• α: 113.043 ± 0.003°
• β: 92.551 ± 0.004°
• γ: 104.67 ± 0.003°
• Cell volume: 2202.2 ± 0.2 ų
• Cell temperature: 173 ± 1 K
• Ambient diffraction temperature: 173 ± 1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1156
• Residual factor for significantly intense reflections: 0.0455
• Weighted residual factors for significantly intense reflections: 0.0693
• Weighted residual factors for all reflections included in the refinement: 0.0766
• Goodness-of-fit parameter for all reflections included in the refinement: 0.775
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No