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Information card for entry 4075220
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Coordinates | 4075220.cif |
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Original paper (by DOI) | HTML |
Common name | 16 |
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Chemical name | Bis[N-(triphenylphosphinimino)phenylacetimidato-N',O]methylsiliconium chloride |
Formula | C58.5 H55.5 Cl11.5 N4 O2.5 P2 Si |
Calculated formula | C58.5 H55.5 Cl11.5 N4 O2.5 P2 Si |
Title of publication | Donor-Stabilized Silyl Cations. 10. Pentacoordinate Siliconium-Ion Salts with a Triphenylphosphinimino-NLigand Group: Two-Bond P−N−Si Coupling as a Measure for Coordination Strength1 |
Authors of publication | Sivaramakrishna, Akella; Kalikhman, Inna; Kertsnus, Evgenia; Korlyukov, Alexander A.; Kost, Daniel |
Journal of publication | Organometallics |
Year of publication | 2006 |
Journal volume | 25 |
Journal issue | 15 |
Pages of publication | 3665 |
a | 14.167 ± 0.004 Å |
b | 16.592 ± 0.003 Å |
c | 17.193 ± 0.004 Å |
α | 61.488 ± 0.004° |
β | 68.668 ± 0.004° |
γ | 83.82 ± 0.006° |
Cell volume | 3297.1 ± 1.4 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1245 |
Residual factor for significantly intense reflections | 0.0637 |
Weighted residual factors for significantly intense reflections | 0.1238 |
Weighted residual factors for all reflections included in the refinement | 0.1369 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4075220.html
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