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Information card for entry 4075238
Preview
Coordinates | 4075238.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C33 H44 Br4 N4 Pd2 |
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Calculated formula | C33 H44 Br4 N4 Pd2 |
Title of publication | Palladium(II) Complexes of a Sterically Bulky, Benzannulated N-Heterocyclic Carbene with Unusual Intramolecular C−H···Pd and Ccarbene···Br Interactions and Their Catalytic Activities |
Authors of publication | Huynh, Han Vinh; Han, Yuan; Ho, Joanne Hui Hui; Tan, Geok Kheng |
Journal of publication | Organometallics |
Year of publication | 2006 |
Journal volume | 25 |
Journal issue | 13 |
Pages of publication | 3267 |
a | 8.6931 ± 0.0006 Å |
b | 9.2111 ± 0.0006 Å |
c | 12.6637 ± 0.0008 Å |
α | 102.509 ± 0.001° |
β | 96.381 ± 0.001° |
γ | 110.548 ± 0.001° |
Cell volume | 907.33 ± 0.1 Å3 |
Cell temperature | 223 ± 2 K |
Ambient diffraction temperature | 223 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0446 |
Residual factor for significantly intense reflections | 0.0312 |
Weighted residual factors for significantly intense reflections | 0.0682 |
Weighted residual factors for all reflections included in the refinement | 0.0733 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.01 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4075238.html
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