Crystallography Open Database

Information card for entry 4075268

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Coordinates	4075268.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H58 Cl N2 P2 Si2 Ti
Calculated formula	C32 H58 Cl N2 P2 Si2 Ti
Title of publication	Terminal Titanium(IV) (Trimethylsilyl)imides Prepared by Oxidatively Induced Trimethylsilyl Abstraction
Authors of publication	Bailey, Brad C.; Basuli, Falguni; Huffman, John C.; Mindiola, Daniel J.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	11
Pages of publication	2725
a	39.26 ± 0.03 Å
b	11.143 ± 0.007 Å
c	17.73 ± 0.013 Å
α	90°
β	106.48 ± 0.07°
γ	90°
Cell volume	7438 ± 10 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0782
Residual factor for significantly intense reflections	0.0448
Weighted residual factors for significantly intense reflections	0.1122
Weighted residual factors for all reflections included in the refinement	0.1295
Goodness-of-fit parameter for all reflections included in the refinement	0.962
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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