Information card for entry 4075436

Structure parameters

• Formula: C26 H63 N4 Si3 Y
• Calculated formula: C26 H63 N4 Si3 Y
• Title of publication: Cationic Group 3 Alkyl Complexes with Isopropyl-Substituted Triazacyclononane-amide Ligands: Synthesis, Structure, and Thermal Decomposition Processes
• Authors of publication: Bambirra, Sergio; Meetsma, Auke; Hessen, Bart; Bruins, Andries P.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 14
• Pages of publication: 3486
• a: 9.9434 ± 0.0006 Å
• b: 17.752 ± 0.001 Å
• c: 19.563 ± 0.001 Å
• α: 91.197 ± 0.001°
• β: 94.254 ± 0.001°
• γ: 91.353 ± 0.001°
• Cell volume: 3441.8 ± 0.3 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.078
• Residual factor for significantly intense reflections: 0.0637
• Weighted residual factors for significantly intense reflections: 0.1446
• Weighted residual factors for all reflections included in the refinement: 0.1516
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No