Information card for entry 4075440

Structure parameters

• Formula: C46 H68 B La N4 O Si
• Calculated formula: C46 H68 B La N4 O Si
• Title of publication: Cationic Group 3 Alkyl Complexes with Isopropyl-Substituted Triazacyclononane-amide Ligands: Synthesis, Structure, and Thermal Decomposition Processes
• Authors of publication: Bambirra, Sergio; Meetsma, Auke; Hessen, Bart; Bruins, Andries P.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 14
• Pages of publication: 3486
• a: 14.573 ± 0.001 Å
• b: 16.465 ± 0.001 Å
• c: 18.963 ± 0.001 Å
• α: 90°
• β: 96.348 ± 0.001°
• γ: 90°
• Cell volume: 4522.2 ± 0.5 ų
• Cell temperature: 200 ± 1 K
• Ambient diffraction temperature: 200 ± 1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1942
• Residual factor for significantly intense reflections: 0.1099
• Weighted residual factors for significantly intense reflections: 0.2623
• Weighted residual factors for all reflections included in the refinement: 0.2929
• Goodness-of-fit parameter for all reflections included in the refinement: 1.521
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No