Information card for entry 4075509

Structure parameters

• Formula: C20 H58 Li2 N4 Si4 Zn
• Calculated formula: C20 H58 Li2 N4 Si4 Zn
• Title of publication: Lithium Dimethyl(amido)zinc Complexes: Contrasting Zincate (Amido = TMP) and Inverse Zincate (Amido = HMDS) Structures on Addition of TMEDA
• Authors of publication: Graham, David V.; Hevia, Eva; Kennedy, Alan R.; Mulvey, Robert E.
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 14
• Pages of publication: 3297
• a: 11.3371 ± 0.0003 Å
• b: 19.7104 ± 0.0005 Å
• c: 15.9168 ± 0.0004 Å
• α: 90°
• β: 103.807 ± 0.002°
• γ: 90°
• Cell volume: 3453.98 ± 0.16 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0586
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0762
• Weighted residual factors for all reflections included in the refinement: 0.0863
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No