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Information card for entry 4075527
Preview
Coordinates | 4075527.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H37 N2 O7 P Si2 W |
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Calculated formula | C23 H37 N2 O7 P Si2 W |
SMILES | [W]([P]1(N=C(N2CCCCC2)C(C1)C(=O)OCC)C([Si](C)(C)C)[Si](C)(C)C)(C#[O])(C#[O])(C#[O])(C#[O])C#[O] |
Title of publication | 1,2-Azaphosphol-5-ene Complexes through Metal-Assisted Synthesis |
Authors of publication | Streubel, Rainer; Wilkens, Hendrik; Ruthe, Frank; Jones, Peter G. |
Journal of publication | Organometallics |
Year of publication | 2006 |
Journal volume | 25 |
Journal issue | 20 |
Pages of publication | 4830 |
a | 10.049 ± 0.003 Å |
b | 17.105 ± 0.004 Å |
c | 17.623 ± 0.01 Å |
α | 90° |
β | 95.5 ± 0.04° |
γ | 90° |
Cell volume | 3015 ± 2 Å3 |
Cell temperature | 143 ± 2 K |
Ambient diffraction temperature | 143 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0422 |
Residual factor for significantly intense reflections | 0.0329 |
Weighted residual factors for significantly intense reflections | 0.0768 |
Weighted residual factors for all reflections included in the refinement | 0.0822 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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