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Information card for entry 4075533
Preview
Coordinates | 4075533.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C13 H30 Cl P Pd |
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Calculated formula | C13 H30 Cl P Pd |
SMILES | [Pd](Cl)(C)[P](C(C)(C)C)(C(C)(C)C)C(C)(C)C |
Title of publication | Syntheses and Structures of Bulky Monophosphine-Ligated Methylpalladium Complexes: Application to Homo- and Copolymerization of Norbornene and/or Methoxycarbonylnorbornene |
Authors of publication | Yamashita, Makoto; Takamiya, Ikuko; Jin, Koichiro; Nozaki, Kyoko |
Journal of publication | Organometallics |
Year of publication | 2006 |
Journal volume | 25 |
Journal issue | 19 |
Pages of publication | 4588 |
a | 8.551 ± 0.009 Å |
b | 9.521 ± 0.009 Å |
c | 9.873 ± 0.011 Å |
α | 91.59 ± 0.02° |
β | 91.034 ± 0.02° |
γ | 94.29 ± 0.02° |
Cell volume | 801.1 ± 1.4 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0322 |
Residual factor for significantly intense reflections | 0.0315 |
Weighted residual factors for significantly intense reflections | 0.0916 |
Weighted residual factors for all reflections included in the refinement | 0.0918 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.213 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4075533.html
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