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Information card for entry 4075564
Preview
Coordinates | 4075564.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C109.5 H101 Cl O7 P6 W2 |
---|---|
Calculated formula | C109.5 H101 Cl O7 P6 W2 |
SMILES | [W]12([P](C#CCCCCCC#C[P]([W]([P](C#CCCCCCC#C[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)([P](C#CCCCCCC#C[P]2(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])(C#[O])C#[O])(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])(C#[O])C#[O].C(Cl)Cl.O(CC)CC |
Title of publication | Synthesis of Ph2PC⋮C(CH2)5C⋮CPPh2Ligand and Its Complexation with Tungsten Carbonyls to Form a Dinuclear Paddle-Wheel and a Tetranuclear Tripodal Compound |
Authors of publication | Shiue, Tsun-Wei; Yeh, Wen-Yann; Lee, Gene-Hsiang; Peng, Shie-Ming |
Journal of publication | Organometallics |
Year of publication | 2006 |
Journal volume | 25 |
Journal issue | 17 |
Pages of publication | 4150 |
a | 21.1762 ± 0.0006 Å |
b | 22.3612 ± 0.0006 Å |
c | 41.0111 ± 0.001 Å |
α | 90° |
β | 90.3001 ± 0.0008° |
γ | 90° |
Cell volume | 19419.5 ± 0.9 Å3 |
Cell temperature | 150 ± 1 K |
Ambient diffraction temperature | 150 ± 1 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0779 |
Residual factor for significantly intense reflections | 0.0478 |
Weighted residual factors for significantly intense reflections | 0.1125 |
Weighted residual factors for all reflections included in the refinement | 0.1272 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4075564.html
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Users of the data should acknowledge the original authors of the
structural data.