Information card for entry 4075602

Structure parameters

• Formula: C44 H67 Cl O2 Os P2 Sn
• Calculated formula: C44 H59 Cl O2 Os P2 Sn
• Title of publication: Preparation, X-ray Structures, and NMR Spectra of Elongated Dihydrogen Complexes with Four- and Five-Coordinate Tin Centers
• Authors of publication: Eguillor, Beatriz; Esteruelas, Miguel A.; Oliván, Montserrat
• Journal of publication: Organometallics
• Year of publication: 2006
• Journal volume: 25
• Journal issue: 19
• Pages of publication: 4691
• a: 10.7119 ± 0.0014 Å
• b: 14.3315 ± 0.0019 Å
• c: 29.82 ± 0.004 Å
• α: 90°
• β: 93.256 ± 0.003°
• γ: 90°
• Cell volume: 4570.5 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1151
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for significantly intense reflections: 0.0807
• Weighted residual factors for all reflections included in the refinement: 0.1074
• Goodness-of-fit parameter for all reflections included in the refinement: 0.789
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No