Information card for entry 4075639

Structure parameters

• Formula: C15 H35 F Ni P2
• Calculated formula: C15 H35 F Ni P2
• SMILES: [Ni]1([P](CC[P]1(C(C)C)C(C)C)(C(C)C)C(C)C)(F)C
• Title of publication: Fluoride Displacement by Lithium Reagents. An Improved Method for the Synthesis of Nickel Hydroxo, Alkoxo, and Amido Complexes
• Authors of publication: Cámpora, Juan; Matas, Inmaculada; Palma, Pilar; Graiff, Claudia; Tiripicchio, Antonio
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 12
• Pages of publication: 2827
• a: 7.727 ± 0.003 Å
• b: 13.228 ± 0.005 Å
• c: 18.666 ± 0.005 Å
• α: 90°
• β: 96.02 ± 0.05°
• γ: 90°
• Cell volume: 1897.4 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.064
• Residual factor for significantly intense reflections: 0.0581
• Weighted residual factors for significantly intense reflections: 0.1701
• Weighted residual factors for all reflections included in the refinement: 0.189
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No